Antimony(III) fluoride: inclusion complexes with crown ethers View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

1996-12

AUTHORS

Janusz Lipkowski, Marina S. Fonari, Victor Ch. Kravtsov, Yurii A. Simonov, Edward V. Ganin, Vladimir O. Gelmboldt

ABSTRACT

Four crystalline molecular complexes between antimony(III) fluoride and 18-membered crown ethers have been obtained and their structures investigated by single crystal X-ray diffraction techniques: [18-crown-6·SbF3], C12H24F3O6Sb,P212121,a=8.328(4),b=11.573(4),c=18.094(4)Å,V=1744(1)Å3,Z=4; [benzo-18-crown-6·SbF3], C16H24F3O6Sb,P21/n,a=10.490(2),b=13.714(1),c=13.442(2)Å, β=101.94(1)°,V=1892(1)Å3,Z=4; [cis-syn-cis-dicyclohexano-18-crown-6·SbF3·CH3OH], C21H40F3O7Sb,P21/n,a=8.270(4),b=23.386(3),c=12.772(1)Å, β=96.31(2)°,V=2455(1)Å3,Z=4; [cis-anti-cis-dicyclohexano-18-crown-6·SbF3], C20H36F3O6Sb,Pna21,a=21.091(8),b=12.829(5),c=8.437(3)Å,V=2283(2)Å3,Z=4. All species are the perching-type complexes with the antimony fluoride above the cavity and the metal lone pair pointed toward the center of the crown ring. The antimony atom interacts with all six crown oxygen atoms with Sb−O distances of 2.837(2)–3.344(2) Å. The antimony atom is displaced from the least square plane of the crown oxygen atoms at the distances of 1.288–1.383 Å. More... »

PAGES

823-833

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/bf01670315

DOI

http://dx.doi.org/10.1007/bf01670315

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1037914389


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