Liquid phase oxidation of transition metals. Part 6. iron and copper complexes containing dimethylsulphoxide, dimethylformamide, and acetonitrile. Anomalous states of ... View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

1980-12

AUTHORS

Igor P. Lavrentiev, Lidia G. Korableva, Elena A. Lavrentieva, Galina A. Nifontova, Mikhail L. Khidekel, Irina G. Gusakovskaya, Tatiana I. Larkina, Levon D. Arutyunian, Olga S. Filipenko, Vasiliy I. Ponomarev, L. O. Atovmyan

ABSTRACT

Direct oxidation of iron and copper in a donor-acceptor medium, L + CCl4, where L is dimethylsulphoxide, dimethylformamide or acetonitrile was employed to obtain complex compounds:cis-[FeCl2(DMSO)4]Cl] (3), 2 FeCl3 · 3 DMSO (5), [FeCl(DMSO)5][FeCl4]2] (6), [FeCl(DMSO)5][Fe2Cl6O] (7),cis-[FeCl2(DMF)4][FeCl4] (8), [Fe(MeCN)6][FeCl4]2 (9) andcis-[CuCl2(DMF)2]2 (10), The structures of complexes (9) and (10) have been established by x-ray diffraction analysis and compared with those of (3), (6), (7) and (8) which are reported elsewhere. The [FeCl(DMSO)5][Fe2Cl6O] complex (7) is formed by oxidation of iron fromcis-[FeIIICl2(DMSO)4]2[FeIICl4] (4) in ethanol. One of the 5 DMSO molecules of (7) was found to be disordered; the Mössbauer spectroscopy data suggest that it can move within the cation coordination sphere. Mössbauer spectroscopy and x-ray diffraction analysis indicate electron isomerism in one of the complexes. More... »

PAGES

193-200

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/bf01396911

DOI

http://dx.doi.org/10.1007/bf01396911

DIMENSIONS

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