X-ray structure of trichloro-oxo-(N-pyridylmethylene-N′-salicyloylhydrazine-NO)molybdenum(V) · acetonitrile (1/1). An example of isomerization by complexation View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

1980-12

AUTHORS

Paolo Domiano, Amos Musatti, Mario Nardelli, Corrado Pelizzi, Giovanni Predieri

ABSTRACT

The synthesis, i.r. spectrum and x-ray crystal structure of the title, complex are described, Crystals are monoclinic space groupP 21/n, witha = 19.901(7),b = 13.163(8),c = 7.273(6) A, β = 90.58(5)° Z = 4, The structure was solved from diffractometer data by direct methods and refined by least-squares techniques toR = 0.053 for 923 independent reflections. The complex has a distortedmer-octahedral geometry [Mo-O = 1,70(1), 2.15(1), Mo-Cl = 2.340(7), 1.352(7), 2.280(7), Mo-N = 2.19(2) A], The starting ligand Hsip, which is in theE configuration when free and in a number of metal complexes where it is terdentate, assumes here theZ configuration and is hiclentate. More... »

PAGES

172-175

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/bf01396904

DOI

http://dx.doi.org/10.1007/bf01396904

DIMENSIONS

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