Crystal structures of bile salts: Sodium taurocholate View Full Text


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Article Info

DATE

1991-10

AUTHORS

Anna Rita Campanelli, Sofia Candeloro De Sanctis, Angelo Antonio D'Archivio, Edoardo Giglio, Lucid Scaramuzza

ABSTRACT

Crystals of sodium taurocholate (NaC26H44NO7S · 2.5 H2O) belonging to the triclinic space groupP1 have unit cell parametersa = 12.731 (2),b = 16.104 (2),c = 7.628 (1) ⫗A, α =83.40 (1),β = 101.20 (1), γ = 105.35 (1)°, and two molecules in the asymmetric unit. The refinement, carried out on 4424 observed reflections, gaveR = 0.059 andRw = 0.066. The packing is characterized by bilayers, formed by antiparallel monolayers and with nonpolar outermost surfaces, held together by van der Waals interactions. Inside the bilayers there are channels, lined with polar groups, and filled by sodium ions and water molecules. A structural unit has been identified that could provide a reasonable model for the micellar aggregates of this bile salt. More... »

PAGES

247-256

References to SciGraph publications

  • 1985-02. Study of the interaction between an optical probe and micelles of sodium deoxycholate in COLLOID AND POLYMER SCIENCE
  • 1960-12. Description of steric relationships across single bonds in CELLULAR AND MOLECULAR LIFE SCIENCES
  • 1991-06. Spectroscopic studies on the interaction between acridine orange and bile salts in JOURNAL OF INCLUSION PHENOMENA AND MACROCYCLIC CHEMISTRY
  • 1991-04. A possible helical model for sodium glycocholate micellar aggregates in JOURNAL OF INCLUSION PHENOMENA AND MACROCYCLIC CHEMISTRY
  • 1989-08. From crystal to micelle: A new approach to the micellar structure in JOURNAL OF INCLUSION PHENOMENA AND MACROCYCLIC CHEMISTRY
  • Identifiers

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    http://scigraph.springernature.com/pub.10.1007/bf01061037

    DOI

    http://dx.doi.org/10.1007/bf01061037

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