Chemical modification of carbon fibres by esterification —optimization of fibre pretreatment View Full Text


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Article Info

DATE

1989-05

AUTHORS

P. D. Jannakoudakis, A. D. Jannakoudakis, E. Theodoridou, J. O. Besenhard

ABSTRACT

Electrochemically oxidized PAN-based carbon fibres were modified by attachment of anm-dinitrobenzene group. Chemical modification was performed by esterification of the −OH groups of the oxidized carbon surface with 3,5-dinitrobenzoyl chloride. The higher modification extent was achieved in the case of d.c. oxidized carbon fibres, which bear a large number of −OH groups. The attachment of the dinitrobenzene species was supported by cyclic voltammetry carried out on the modified carbon fibre electrodes in aqueous solutions. The quantity of attachedm-dinitrobenzene groups was determined polarographically, after hydrolysis of the esteric bonds; it corresponds to a charge density of ca 0.2 kAh kg−1 carbon fibres, which is of the order of magnitude of battery electrodes. More... »

PAGES

341-344

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/bf01015233

DOI

http://dx.doi.org/10.1007/bf01015233

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1004614947


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