Synthesis, structure, and magnetic properties of iron — yttrium complexes containing acetylacetonate ligands View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

1995-08

AUTHORS

M. V. Tsodikov, O. V. Bukhtenko, O. G. Ellert, I. A. Petrunenko, A. S. Antsyshkina, G. G. Sadikov, Yu. V. Maksimov, Yu. V. Titov, V. M. Novotortsev

ABSTRACT

Two new compounds have been obtained by the synthesis of heteronuclear iron-yttrium acetylacetonate, using the modified electrochemical dissolution of the [YFe2] alloy. One of these compounds, with the Fe(acac)2 · 2H2O composition, has been studied by X-ray diffraction analysis. X-ray diffraction data: a=11.002(5), b=5.412(2), c=11.179(5) Å;β=106.39(4)°;V=638.6 Å3, space group P21/c, Z=2. According to the data on magnetic susceptibility, Mössbauer spectroscopy, and X-ray electron microanalysis, single crystals of this complex are covered with an amorphous film containing finely dispersed [Y1−aFea]n clusters and, probably, superparamagnetic γ-Fe2O3 species. The second oligomeric acetylacetonate complex contains ions of high-spin two-valence iron, yttrium, and finely dispersed ferromagnetic [Y1−aFea)n intermetallide clusters. More... »

PAGES

1396-1400

References to SciGraph publications

Journal

TITLE

Russian Chemical Bulletin

ISSUE

8

VOLUME

44

Author Affiliations

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/bf00714416

DOI

http://dx.doi.org/10.1007/bf00714416

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1015301492


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