An X-ray study of a 12-crown-4 host-guest complex. Crystal structure of the 4∶6 complex between 12-crown-4 and aminosulfuric acid View Full Text


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Article Info

DATE

1993-12

AUTHORS

Yurii A. Simonov, Marina S. Fonari, Alexander A. Dvorkin, Tadeush I. Malinovski, Janusz Lipkowski, Edward V. Ganin

ABSTRACT

The title compound was prepared by treating a methanolic solution of 12-crown-4 with an aqueous solution of aminosulfuric acid. The crystal for X-ray analysis was obtained by recrystallization from acetone. The compound [(12-crown-4)4·[NH3SO3)6] (1) is monoclinic, space groupP21/a,a=21.900(8),b=15.499(5),c=18.079(5) Å, γ=67.85(2)°. Refinement led to a final conventionalR value of 0.0788 for 3280 reflections. More... »

PAGES

315-327

References to SciGraph publications

  • 1986-12. f-Element/crown ether complexes 2. The synthesis and crystal structure of Y(NO3)3(12-crown-4) in JOURNAL OF INCLUSION PHENOMENA AND MACROCYCLIC CHEMISTRY
  • 1984-03. From crown ethers to zeolites: Reaction of EtAlCl2 with crown ethers in JOURNAL OF INCLUSION PHENOMENA AND MACROCYCLIC CHEMISTRY
  • 1990-10. Crystal structures of inclusion compounds of 4-aminobenzenesulfamidine (sulfaguanidine) with two dicyclohexano-18-crown-6 isomers in JOURNAL OF INCLUSION PHENOMENA AND MACROCYCLIC CHEMISTRY
  • 1989-12. Inclusion compounds ofcis-syn-cis andcis-anti-cis diastereoisomers of dicyclohexano-18-crown-6 with amidosulfuric acid in JOURNAL OF INCLUSION PHENOMENA AND MACROCYCLIC CHEMISTRY
  • 1991-07. The 1 : 1 complexes between benzo-18-crown-6, 18-crown-6 and aminosulfuric acid in JOURNAL OF INCLUSION PHENOMENA AND MACROCYCLIC CHEMISTRY
  • 1991-10. Conformational analysis of 12-crown-4 in JOURNAL OF INCLUSION PHENOMENA AND MACROCYCLIC CHEMISTRY
  • Identifiers

    URI

    http://scigraph.springernature.com/pub.10.1007/bf00708712

    DOI

    http://dx.doi.org/10.1007/bf00708712

    DIMENSIONS

    https://app.dimensions.ai/details/publication/pub.1020696301


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