Twelve-membered crown ethers: Crystal structures of benzo-12-crown-4 and naphtho-12-crown-4 View Full Text


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Article Info

DATE

1993-03

AUTHORS

Yurii A. Simonov, Alexandr A. Dvorkin, Marina S. Fonari, Tadeush I. Malinowski, Elżbieta Luboch, Andrzej Cygan, Jan F. Biernat, Edward V. Ganin, Yurii A. Popkov

ABSTRACT

The crystal structures of two 12-membered crown ethers, benzo-12-crown-4 (1) and naphtho-12-crown-4 (2), have been determined by X-ray analysis. Both structures are molecular. Compound1 is monoclonic,P21/b,a=8.466(3),b=8.019(3),c=33.590(10) Å, γ=90.99(3)o. The unit cell contains two crystallographically independent molecules of1 with similar conformations. Compound2 is also monoclinic,P21/a,a=24.148(8),b=14.535(4),c=7.987(5) Å, γ=102.87(2)o. Two independent molecules in the unit cell have significantly different conformations. More... »

PAGES

79-89

References to SciGraph publications

  • 1991-10. Conformational analysis of 12-crown-4 in JOURNAL OF INCLUSION PHENOMENA AND MACROCYCLIC CHEMISTRY
  • Identifiers

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    http://scigraph.springernature.com/pub.10.1007/bf00706476

    DOI

    http://dx.doi.org/10.1007/bf00706476

    DIMENSIONS

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