Structural researches on metal complexes with ligands containing the pyridoxal moiety: X-ray structure of chloro(N-pyridoxylidene-N′-salicyloylhydrazinato) copper(II) Monohydrate View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

1979-12

AUTHORS

Paolo Domiano, Amos Musatti, Mario Nardelli, Corrado Pelizzi, Giovanni Predieri

ABSTRACT

The x-ray crystal structure of the title complex is described Crystals are monoclinic, space groupP21/n, with unit-cell dimensions:a=18.070(2),b=13.471(2),c=6.788(2) Å,β=94.70(1)∘,Z=4. The structure was solved from diffractometer data by Patterson and Fourier methods and refined by least-squares techniques toR=5.0% for 2451 independent reflections. It consists of complex molecules, in which the copper atom square planar coordination comprises the chlorine atom, Cu-Cl=2.240(3) Å, and the organic ligand which acts as terdentate through the oxygen atom [Cu-O=1.948(3) Å] and a nitrogen atom, [Cu-N=1.933(5) Å] from the hydrazidic chain and the oxygen atom, [Cu-O = 1.894(4) Å] from the pyridoxal group. More... »

PAGES

351-354

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/bf00623975

DOI

http://dx.doi.org/10.1007/bf00623975

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1027386548


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