Kinetic- and catalytic-spectrophotometric determination of iron by pyrogallolphthalein and potassium perdisulphate in non-ionic surfactant micellar medium View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

1989-01

AUTHORS

I. Mori, Y. Fujita, K. Ikuta, Y. Nakahashi, K. Kato, K. Tamura, M. Ohji

ABSTRACT

A simple and highly sensitive spectrophotometric determination of iron with pyrogallolphthalein in a micellar medium of non-ionic surfactant is proposed. This method is based on the kinetic-catalytic action of iron(III) upon the decomposition reaction between pyrogallolphthalein and potassium perdisulphate at pH 2.4–2.9 in the presence of Triton X 100 as a non-ionic surfactant. The calibration graph is linear over the range 10–600 ng iron(III) per 10 ml in spectrophotometry (apparent molar absorption coefficient for decomposition was 1.25×10−6 l per mole per cm at 385 nm). The method was applied to assay and recovery tests for artificial waste water with satisfactory results (recovery 97.6%–103.5%). More... »

PAGES

49-52

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/bf00481972

DOI

http://dx.doi.org/10.1007/bf00481972

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1019479647


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