Crystallinity of cellulose, as determined by CP/MAS NMR and XRD methods View Full Text


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Article Info

DATE

1987-03

AUTHORS

R. Teeäär, R. Serimaa, T. Paakkarl

ABSTRACT

The crystallinity of six cellulose samples with different origin and treatment was determined using x-ray diffraction (XDR) and nuclear magnetic resonance with cross polarization and magic angle sample spinning (CP/MAS NMR) methods. The numerical results for crystallinity obtained by using curve fitting methods in both cases correlated very well. It was concluded that the values for the crystallinity can be determined from NMR spectra when CP times not exceeding 0.5 ms are used. The range of order of the samples was further characterized calculating the radial atomic density function from the x-ray diffraction patterns and determining the greatest distances with significant deviations from the average density. More... »

PAGES

231-237

References to SciGraph publications

Journal

TITLE

Polymer Bulletin

ISSUE

3

VOLUME

17

Author Affiliations

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/bf00285355

DOI

http://dx.doi.org/10.1007/bf00285355

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1000980360


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