A general enhancement scheme in heteronuclear multidimensional NMR employing pulsed field gradients View Full Text


Ontology type: schema:ScholarlyArticle     


Article Info

DATE

1994-03

AUTHORS

J. Schleucher, M. Schwendinger, M. Sattler, P. Schmidt, O. Schedletzky, S. J. Glaser, O. W. Sørensen, C. Griesinger

ABSTRACT

General pulse sequence elements that achieve sensitivity-enhanced coherence transfer from a heteronucleus to protons of arbitrary multiplicity are introduced. The building blocks are derived from the sensitivity-enhancement scheme introduced by Cavanagh et al. ((1991) J. Magn. Reson., 91, 429-436), which was used in conjunction with gradient coherence selection by Kay et al. ((1992) J. Am. Chem. Soc., 114, 10663-10665), as well as from a multiple-pulse sequence effecting a heteronuclear planar coupling Hamiltonian. The building blocks are incorporated into heteronuclear correlation experiments, in conjunction with coherence selection by the formation of a heteronuclear gradient echo. This allows for efficient water suppression without the need for water presaturation. The methods are demonstrated in HSQC-type experiments on a sample of a decapeptide in H2O. The novel pulse sequence elements can be incorporated into multidimensional experiments. More... »

PAGES

301-306

References to SciGraph publications

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/bf00175254

DOI

http://dx.doi.org/10.1007/bf00175254

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1009330408

PUBMED

https://www.ncbi.nlm.nih.gov/pubmed/8019138


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