Hydrodynamics of Centrifugal Partition Chromatography View Full Text


Ontology type: schema:Chapter     


Chapter Info

DATE

1993

AUTHORS

R. Meester , M. J. van Buel , L. A. M. van der Wielen , R. Verpoorte , K. Ch. A. M. Luyben

ABSTRACT

The hydrodynamics of Centrifugal Partition Chromatography (CPC), an interesting analytical and preparative scale separation technique, are being investigated for modelling and scale-up. The influences of input variables on hold-up and pressure drop have been measured with an analytical scale CP-chromatograph; a preliminary overview of the first results is given. It is assumed that a number of flow regimes are possible. The formation of individual droplets of mobile phase in the stationary phase is questionable; it is more likely that jets and bypasses are formed. The maximal hold-up of the stationary phase in an analytical scale CPC-column is affected by flow rate and centrifugal field; more stationary phase (up to 73 vol. %) can be retained when the rotation frequency is increased, while the stationary phase hold-up gradually decreases with increasing flow rate. More... »

PAGES

295-303

Book

TITLE

Precision Process Technology

ISBN

978-94-010-4772-2
978-94-011-1759-3

Author Affiliations

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/978-94-011-1759-3_22

DOI

http://dx.doi.org/10.1007/978-94-011-1759-3_22

DIMENSIONS

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