Challenges in Detection, Structural Characterization and Determination of Complex Formation Constants of Uranyl-Arsenate Complexes in Aqueous Solutions View Full Text


Ontology type: schema:Chapter     


Chapter Info

DATE

2011

AUTHORS

Wondemagegnehu A. Gezahegne , Christoph Hennig , Gerhard Geipel , Britta Planer-Friedrich , Broder J. Merkel

ABSTRACT

Uranium forms analogous minerals with phosphate and arsenate. In aqueous solutions an analogy is expected to govern the complexes that uranium builds with these ligands. Three uranyl arsenate complexes UO2H2AsO4+, UO2HAsO40 and UO2(H2AsO4)20 were identified and reported previously with TRLFS in the pH range 1 to 3. Using a similar detection system and elevating the pH range a negatively charged fourth uranyl-arsenate complex, UO2AsO4− was found under circum neutral pH. Determining the complex formation constant for this complex was not possible due to the susceptibility of the fluorescence intensity to external influences and the difficulty of resolving the measured spectra into individual fluorescence contributions. By immediate shock-freezing to 15 K we succeeded to measure a reproducible EXAFS spectrum of a uranyl-arsenate species in an aqueous solution at pH 2. More... »

PAGES

607-616

References to SciGraph publications

  • 1986. EXAFS: Basic Principles and Data Analysis in NONE
  • 1992. Electronic structure and bonding in actinyl ions in COMPLEXES, CLUSTERS AND CRYSTAL CHEMISTRY
  • 1997-10. Uranium(VI) speciation by spectroscopy in JOURNAL OF RADIOANALYTICAL AND NUCLEAR CHEMISTRY
  • Book

    TITLE

    The New Uranium Mining Boom

    ISBN

    978-3-642-22121-7
    978-3-642-22122-4

    Identifiers

    URI

    http://scigraph.springernature.com/pub.10.1007/978-3-642-22122-4_70

    DOI

    http://dx.doi.org/10.1007/978-3-642-22122-4_70

    DIMENSIONS

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