Bottom-Up Fabrication of Two-Dimensional Polymers on Solid Surfaces View Full Text


Ontology type: schema:Chapter     


Chapter Info

DATE

2016

AUTHORS

Markus Lackinger

ABSTRACT

Two-dimensional polymers are a novel class of future materials that are not purely hypothetical anymore, but have not been realized in full yet. A promising and versatile synthetic approach is the bottom-up fabrication by polymerization of monomers into covalently cross-linked nanostructures on solid surfaces. This chapter introduces the synthetic approach consisting of monomer deposition and activation, and describes a typical characterization scheme by established surface science techniques—high-resolution Scanning Tunneling Microscopy for structures and X-ray Photoelectron Spectroscopy for chemical state. The coupling chemistry is largely predetermined by monomer functionalization and various coupling reactions can be utilized to achieve cross-linking on surfaces. A major aim of this chapter is to compare and discuss the most popular interlinking chemistry and to highlight important implications when classical reactions are transferred from a beaker to a solid surface. The most important distinction is whether coupling proceeds irreversibly and remains kinetically controlled or whether thermodynamical control is possible. Ullmann coupling is a prominent example for an irreversible reaction. Recent achievements with focus on defect formation as well as the occurrence and utility of organometallic intermediates are discussed. Long-range ordered covalent organic frameworks were demonstrated based on boronic acid condensation. In this context, emphasis will be put on the importance of bond reversibility. Moreover, coupling reactions of terminal alkynes are introduced, and both possibilities and limitations are illustrated by referring to recent examples. More... »

PAGES

199-219

Book

TITLE

On-Surface Synthesis

ISBN

978-3-319-26598-8
978-3-319-26600-8

Author Affiliations

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/978-3-319-26600-8_10

DOI

http://dx.doi.org/10.1007/978-3-319-26600-8_10

DIMENSIONS

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50 schema:description Two-dimensional polymers are a novel class of future materials that are not purely hypothetical anymore, but have not been realized in full yet. A promising and versatile synthetic approach is the bottom-up fabrication by polymerization of monomers into covalently cross-linked nanostructures on solid surfaces. This chapter introduces the synthetic approach consisting of monomer deposition and activation, and describes a typical characterization scheme by established surface science techniques—high-resolution Scanning Tunneling Microscopy for structures and X-ray Photoelectron Spectroscopy for chemical state. The coupling chemistry is largely predetermined by monomer functionalization and various coupling reactions can be utilized to achieve cross-linking on surfaces. A major aim of this chapter is to compare and discuss the most popular interlinking chemistry and to highlight important implications when classical reactions are transferred from a beaker to a solid surface. The most important distinction is whether coupling proceeds irreversibly and remains kinetically controlled or whether thermodynamical control is possible. Ullmann coupling is a prominent example for an irreversible reaction. Recent achievements with focus on defect formation as well as the occurrence and utility of organometallic intermediates are discussed. Long-range ordered covalent organic frameworks were demonstrated based on boronic acid condensation. In this context, emphasis will be put on the importance of bond reversibility. Moreover, coupling reactions of terminal alkynes are introduced, and both possibilities and limitations are illustrated by referring to recent examples.
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