Neutron Diffraction Investigation of Hexagonal and Cubic Phases of System Ti-C-H View Full Text


Ontology type: schema:Chapter     


Chapter Info

DATE

2009-01-01

AUTHORS

I. Khidirov , B. B. Mirzaev , N. N. Mukhtarova , KH. M. Kholmedov , S. YU. Zaginaichenko , D. V. Schur

ABSTRACT

It is established that at hardening from 1,000°C in samples TiCxHy at the concentration of carbon of 0.30 ≤ x ≤ 0.50 and at a ratio y ≥ x the ordered hexagonal close-packed (HCP)-structure and at y < x — face-centered cubic (FCC)-phase are stabilized. The crystal structure of the ordered HCP-phase corresponding to the formula Ti2C1-x′ H2-y′ (1-x′ = 2x; 2-y′ = 2y) is described in the framework of sp. gr. P3m1. Below 700°C the Ti2C1-x′H2-y′ -phase with concentration of carbon 0.30 ≤ x < 0.41 decayed with precipitation of the hydride phase TiH2. The ordered solid solution Ti2C1-x′ H2-y′ is stable at concentration 0.41 > C/Ti > 0.50 (close to stoichiometry on carbon Ti2C) but is metastable at concentrations 0.30 > C/Ti > 0.41. Compounds TiCxHy at concentrations 0.45 ≤ x ≤ 0.50 and y < x have both disordered (sp. gr. Fm3m) and ordered FCC-structure (sp. gr.Fd3m) depending on temperature.Cubic carbohydride TiC0.47H0.22 was prepared by means of quenching from 1,200°C followed by heat treatment using special regime for preventing the exit of hydrogen out of the lattice. It is shown that at the lower limit of homogeneity range of the cubic carbohydride hydrogen atoms occupy tetrahedral interstices 8(c) of the disordered cubic structure (sp. gr. Fm3m). It is found that carbon and hydrogen atoms are partially ordered when annealing at 900–800°C. In the ordered phase (sp. gr. Fd3m) carbon atoms occupy mainly (70%) octahedral interstices 16(c ) and 30% of carbon and the most part of hydrogen atoms — another type of octahedral interstices 16(d). More... »

PAGES

663-678

Identifiers

URI

http://scigraph.springernature.com/pub.10.1007/978-1-4020-8898-8_83

DOI

http://dx.doi.org/10.1007/978-1-4020-8898-8_83

DIMENSIONS

https://app.dimensions.ai/details/publication/pub.1033123685


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