2008
AUTHORSA. D. Pomogailo , A. S. Rozenberg , G. I. Dzhardimalieva , A. M. Bochkin , S. I. Pomogailo , N. D. Golubeva
ABSTRACTNew types of hafnium-containing nanocomposites were prepared by combining polymer synthesis and controlled thermolysis. This approach involved the preparation and subsequent thermolysis of hafnium-containing polymers or concurrent solid-state polymerization of hafnium-containing monomers and thermal decomposition of the forming metal-containing polymer at different temperatures. The composition and structure of the synthesized hafnium-containing precursors and thermolysis products are determined by elemental analysis, IR spectroscopy, mass spectrometry, optical microscopy, and x-ray diffraction. Thermodynamic analysis was used to assess the equilibrium composition of the Hf-C-H-O system and establish the conditions under which HfC and HfO2 were formed. More... »
PAGES241-267
Inorganic and Organometallic Macromolecules
ISBN
978-0-387-72946-6
978-0-387-72947-3
http://scigraph.springernature.com/pub.10.1007/978-0-387-72947-3_10
DOIhttp://dx.doi.org/10.1007/978-0-387-72947-3_10
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