Silver ion chromatography of high purity conjugated linoleic acid (CLA)


Ontology type: sgo:Patent     


Patent Info

DATE

2000-11-28T00:00

AUTHORS

Michael C. Seidel

ABSTRACT

A method for providing a purified conjugated linoleic acid (CLA) is disclosed. The purified conjugated linoleic acid (CLA) is formed by separating by liquid chromatography a 9-cis, 11-trans octadecadienoic acid formed by a novel synthesis of reacting an ester of ricinoleic acid with a tosyl chloride or a mesyl chloride to form a tosylate or mesylate of an ester of ricinoleic acid, and reacting the tosylate or mesylate of an ester of ricinoleic acid with diazabicyclo-undecene. Reacting an ester of ricinoleic acid with a tosyl chloride or a mesyl chloride to form a tosylate or mesylate of an ester of ricinoleic acid, and reacting the tosylate or mesylate of an ester of ricinoleic acid with diazabicyclo-undecene forms a 9-cis, 11-trans octadecadienoic acid having a purity greater than 50%, and separating by liquid chromatography forms a 9-cis, 11-trans octadecadienoic acid having a purity greater than 90%. In one aspect, the liquid chromatography uses a strong acid macroreticular ion exchange resin. In one aspect, the liquid chromatography includes silver ion liquid chromatography. More... »

JSON-LD is the canonical representation for SciGraph data.

TIP: You can open this SciGraph record using an external JSON-LD service: JSON-LD Playground Google SDTT

[
  {
    "@context": "https://springernature.github.io/scigraph/jsonld/sgcontext.json", 
    "about": [
      {
        "id": "http://purl.org/au-research/vocabulary/anzsrc-for/2008/2428", 
        "inDefinedTermSet": "http://purl.org/au-research/vocabulary/anzsrc-for/2008/", 
        "type": "DefinedTerm"
      }
    ], 
    "author": [
      {
        "name": "Michael C. Seidel", 
        "type": "Person"
      }
    ], 
    "citation": [
      {
        "id": "https://doi.org/10.1016/0021-9150(94)90034-5", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1003660255"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "sg:pub.10.1007/s11746-997-0018-z", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1009182792", 
          "https://doi.org/10.1007/s11746-997-0018-z"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "sg:pub.10.1007/s11745-997-0156-3", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1019739405", 
          "https://doi.org/10.1007/s11745-997-0156-3"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "sg:pub.10.1007/s11746-997-0203-0", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1036190836", 
          "https://doi.org/10.1007/s11746-997-0203-0"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "sg:pub.10.1007/s11745-998-0236-4", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1037031989", 
          "https://doi.org/10.1007/s11745-998-0236-4"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "sg:pub.10.1007/s11745-998-0198-6", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1037367052", 
          "https://doi.org/10.1007/s11745-998-0198-6"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "https://doi.org/10.1006/bbrc.1998.8303", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1041640394"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "https://doi.org/10.1016/0009-3084(71)90026-0", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1041845071"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "https://doi.org/10.1016/0009-3084(71)90026-0", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1041845071"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "sg:pub.10.1007/bf02662205", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1044488910", 
          "https://doi.org/10.1007/bf02662205"
        ], 
        "type": "CreativeWork"
      }, 
      {
        "id": "sg:pub.10.1007/s11745-998-0223-9", 
        "sameAs": [
          "https://app.dimensions.ai/details/publication/pub.1052960104", 
          "https://doi.org/10.1007/s11745-998-0223-9"
        ], 
        "type": "CreativeWork"
      }
    ], 
    "datePublished": "2000-11-28T00:00", 
    "description": "

A method for providing a purified conjugated linoleic acid (CLA) is disclosed. The purified conjugated linoleic acid (CLA) is formed by separating by liquid chromatography a 9-cis, 11-trans octadecadienoic acid formed by a novel synthesis of reacting an ester of ricinoleic acid with a tosyl chloride or a mesyl chloride to form a tosylate or mesylate of an ester of ricinoleic acid, and reacting the tosylate or mesylate of an ester of ricinoleic acid with diazabicyclo-undecene. Reacting an ester of ricinoleic acid with a tosyl chloride or a mesyl chloride to form a tosylate or mesylate of an ester of ricinoleic acid, and reacting the tosylate or mesylate of an ester of ricinoleic acid with diazabicyclo-undecene forms a 9-cis, 11-trans octadecadienoic acid having a purity greater than 50%, and separating by liquid chromatography forms a 9-cis, 11-trans octadecadienoic acid having a purity greater than 90%. In one aspect, the liquid chromatography uses a strong acid macroreticular ion exchange resin. In one aspect, the liquid chromatography includes silver ion liquid chromatography.

", "id": "sg:patent.US-6153774-A", "keywords": [ "ion chromatography", "conjugated linoleic acid", "method", "liquid chromatography", "trans", "novel synthesis", "ester", "acid", "chloride", "purity", "aspect", "ion exchange resin" ], "name": "Silver ion chromatography of high purity conjugated linoleic acid (CLA)", "sameAs": [ "https://app.dimensions.ai/details/patent/US-6153774-A" ], "sdDataset": "patents", "sdDatePublished": "2019-04-18T10:27", "sdLicense": "https://scigraph.springernature.com/explorer/license/", "sdPublisher": { "name": "Springer Nature - SN SciGraph project", "type": "Organization" }, "sdSource": "s3://com-uberresearch-data-patents-target-20190320-rc/data/sn-export/402f166718b70575fb5d4ffe01f064d1/0000100128-0000352499/json_export_03082.jsonl", "type": "Patent" } ]
 

Download the RDF metadata as:  json-ld nt turtle xml License info

HOW TO GET THIS DATA PROGRAMMATICALLY:

JSON-LD is a popular format for linked data which is fully compatible with JSON.

curl -H 'Accept: application/ld+json' 'https://scigraph.springernature.com/patent.US-6153774-A'

N-Triples is a line-based linked data format ideal for batch operations.

curl -H 'Accept: application/n-triples' 'https://scigraph.springernature.com/patent.US-6153774-A'

Turtle is a human-readable linked data format.

curl -H 'Accept: text/turtle' 'https://scigraph.springernature.com/patent.US-6153774-A'

RDF/XML is a standard XML format for linked data.

curl -H 'Accept: application/rdf+xml' 'https://scigraph.springernature.com/patent.US-6153774-A'


 

This table displays all metadata directly associated to this object as RDF triples.

69 TRIPLES      14 PREDICATES      35 URIs      20 LITERALS      2 BLANK NODES

Subject Predicate Object
1 sg:patent.US-6153774-A schema:about anzsrc-for:2428
2 schema:author N07034fd958f8448cabb8ae1473ab3891
3 schema:citation sg:pub.10.1007/bf02662205
4 sg:pub.10.1007/s11745-997-0156-3
5 sg:pub.10.1007/s11745-998-0198-6
6 sg:pub.10.1007/s11745-998-0223-9
7 sg:pub.10.1007/s11745-998-0236-4
8 sg:pub.10.1007/s11746-997-0018-z
9 sg:pub.10.1007/s11746-997-0203-0
10 https://doi.org/10.1006/bbrc.1998.8303
11 https://doi.org/10.1016/0009-3084(71)90026-0
12 https://doi.org/10.1016/0021-9150(94)90034-5
13 schema:datePublished 2000-11-28T00:00
14 schema:description <p>A method for providing a purified conjugated linoleic acid (CLA) is disclosed. The purified conjugated linoleic acid (CLA) is formed by separating by liquid chromatography a 9-cis, 11-trans octadecadienoic acid formed by a novel synthesis of reacting an ester of ricinoleic acid with a tosyl chloride or a mesyl chloride to form a tosylate or mesylate of an ester of ricinoleic acid, and reacting the tosylate or mesylate of an ester of ricinoleic acid with diazabicyclo-undecene. Reacting an ester of ricinoleic acid with a tosyl chloride or a mesyl chloride to form a tosylate or mesylate of an ester of ricinoleic acid, and reacting the tosylate or mesylate of an ester of ricinoleic acid with diazabicyclo-undecene forms a 9-cis, 11-trans octadecadienoic acid having a purity greater than 50%, and separating by liquid chromatography forms a 9-cis, 11-trans octadecadienoic acid having a purity greater than 90%. In one aspect, the liquid chromatography uses a strong acid macroreticular ion exchange resin. In one aspect, the liquid chromatography includes silver ion liquid chromatography.</p>
15 schema:keywords acid
16 aspect
17 chloride
18 conjugated linoleic acid
19 ester
20 ion chromatography
21 ion exchange resin
22 liquid chromatography
23 method
24 novel synthesis
25 purity
26 trans
27 schema:name Silver ion chromatography of high purity conjugated linoleic acid (CLA)
28 schema:sameAs https://app.dimensions.ai/details/patent/US-6153774-A
29 schema:sdDatePublished 2019-04-18T10:27
30 schema:sdLicense https://scigraph.springernature.com/explorer/license/
31 schema:sdPublisher N8231828788174f5ca7a50b0757d6feda
32 sgo:license sg:explorer/license/
33 sgo:sdDataset patents
34 rdf:type sgo:Patent
35 N07034fd958f8448cabb8ae1473ab3891 rdf:first Nb4238d4cd2fa4a189cf86561786d6b17
36 rdf:rest rdf:nil
37 N8231828788174f5ca7a50b0757d6feda schema:name Springer Nature - SN SciGraph project
38 rdf:type schema:Organization
39 Nb4238d4cd2fa4a189cf86561786d6b17 schema:name Michael C. Seidel
40 rdf:type schema:Person
41 anzsrc-for:2428 schema:inDefinedTermSet anzsrc-for:
42 rdf:type schema:DefinedTerm
43 sg:pub.10.1007/bf02662205 schema:sameAs https://app.dimensions.ai/details/publication/pub.1044488910
44 https://doi.org/10.1007/bf02662205
45 rdf:type schema:CreativeWork
46 sg:pub.10.1007/s11745-997-0156-3 schema:sameAs https://app.dimensions.ai/details/publication/pub.1019739405
47 https://doi.org/10.1007/s11745-997-0156-3
48 rdf:type schema:CreativeWork
49 sg:pub.10.1007/s11745-998-0198-6 schema:sameAs https://app.dimensions.ai/details/publication/pub.1037367052
50 https://doi.org/10.1007/s11745-998-0198-6
51 rdf:type schema:CreativeWork
52 sg:pub.10.1007/s11745-998-0223-9 schema:sameAs https://app.dimensions.ai/details/publication/pub.1052960104
53 https://doi.org/10.1007/s11745-998-0223-9
54 rdf:type schema:CreativeWork
55 sg:pub.10.1007/s11745-998-0236-4 schema:sameAs https://app.dimensions.ai/details/publication/pub.1037031989
56 https://doi.org/10.1007/s11745-998-0236-4
57 rdf:type schema:CreativeWork
58 sg:pub.10.1007/s11746-997-0018-z schema:sameAs https://app.dimensions.ai/details/publication/pub.1009182792
59 https://doi.org/10.1007/s11746-997-0018-z
60 rdf:type schema:CreativeWork
61 sg:pub.10.1007/s11746-997-0203-0 schema:sameAs https://app.dimensions.ai/details/publication/pub.1036190836
62 https://doi.org/10.1007/s11746-997-0203-0
63 rdf:type schema:CreativeWork
64 https://doi.org/10.1006/bbrc.1998.8303 schema:sameAs https://app.dimensions.ai/details/publication/pub.1041640394
65 rdf:type schema:CreativeWork
66 https://doi.org/10.1016/0009-3084(71)90026-0 schema:sameAs https://app.dimensions.ai/details/publication/pub.1041845071
67 rdf:type schema:CreativeWork
68 https://doi.org/10.1016/0021-9150(94)90034-5 schema:sameAs https://app.dimensions.ai/details/publication/pub.1003660255
69 rdf:type schema:CreativeWork
 




Preview window. Press ESC to close (or click here)


...